5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid

Base Information

• Chemical Name: 5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid
• CAS No.: 166319-91-1
• Molecular Formula: C₂₁H₃Cl₁₃O₄
• Molecular Weight: 780.141
• Mol file: 166319-91-1.mol

Synonyms:5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid

Chemical Property of 5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid

Chemical Property:

Purity/Quality:

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Technology Process of 5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid

There total 1 articles about 5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5--2,4,6-trichlorobenzene-1,3-dicarboxyaldehyde → 5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid (166319-91-1)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In water; acetone; Ambient temperature;

DOI:10.1016/0040-4020(95)00353-A

Reference yield: 52.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid (166319-91-1) → dimethyl 5--2,4,6-trichlorobenzene-1,3-dicarboxylate

Guidance literature:

In diethyl ether;

DOI:10.1016/0040-4020(95)00353-A

Reference yield:

5--2,4,6-trichlorobenzene-1,3-dicarboxylic acid (166319-91-1) → (3,5-dicarboxy-2,4,6-trichlorophenyl)bis(pentachlorophenyl)methyl radical

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; chloranil; Yield given. Multistep reaction; 1.) THF, H₂O, r.t., 18 h; 2.) THF, H₂O, r.t., 2 h;

DOI:10.1016/0040-4020(95)00353-A