2'-Phenylethyl 2-methyl-2-propenesulfonate

Base Information

Chemical Name:2'-Phenylethyl 2-methyl-2-propenesulfonate
CAS No.:125452-88-2
Molecular Formula:C₁₂H₁₆O₃S
Molecular Weight:240.323
Hs Code.:

Synonyms:2'-Phenylethyl 2-methyl-2-propenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-Phenylethyl 2-methyl-2-propenesulfonate

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Technology Process of 2'-Phenylethyl 2-methyl-2-propenesulfonate

There total 2 articles about 2'-Phenylethyl 2-methyl-2-propenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 125452-81-5
2-Phenylethyl 2-methylallyl sulfite

: 125452-88-2
2'-Phenylethyl 2-methyl-2-propenesulfonate

Guidance literature:: [Pd₂(dba)₃]*benzene; triethyl phosphite; In 1,4-dioxane; for 45h; Ambient temperature;
DOI:10.1021/jo00293a028

Reference yield:

: 33681-75-3
2-Phenylethyl chlorosulfite

: 125452-88-2
2'-Phenylethyl 2-methyl-2-propenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-BuLi / 1) THF, -78 deg C, 10 min; 2) 1 h,

2: 77 percent / (dba)3Pd₂C₆H₆, triethyl phosphite / dioxane / 45 h / Ambient temperature

With n-butyllithium; [Pd₂(dba)₃]*benzene; triethyl phosphite; In 1,4-dioxane;
DOI:10.1021/jo00293a028