7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine

Base Information

• Chemical Name: 7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine
• CAS No.: 106362-96-3
• Molecular Formula: C₁₅H₁₅ClN₄O₂S
• Molecular Weight: 350.829

Synonyms:7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine

Chemical Property of 7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine

Chemical Property:

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Technology Process of 7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine

There total 2 articles about 7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

3-methyl-4-amino-5-mercapto-1,2,4-triazole (20939-15-5) + 3-bromo-4-(4-chloro-phenyl)-4-oxo-butyric acid ethyl ester (35158-46-4) → 7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine (106362-96-3)

Guidance literature:

In ethanol; for 24h; Heating;

Reference yield:

ethyl 4-(4-chlorophenyl)-4-oxobutanoate (53503-49-4) → 7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine (106362-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / Br₂, anh. AlCl₃ / CHCl₃

2: 60 percent / ethanol / 24 h / Heating

With aluminium trichloride; bromine; In ethanol; chloroform;

Reference yield: 80.0%

7-carbethoxymethyl-6-(p-chlorophenyl)-3-methyl-s-triazolo<3,4-b><1,3,4>thiadiazine (106362-96-3) → [6-(4-Chloro-phenyl)-3-methyl-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazin-7-yl]-acetic acid (106363-05-7)

Guidance literature:

With sodium hydroxide; In methanol; for 1h; Heating;

upstream raw materials:

3-methyl-4-amino-5-mercapto-1,2,4-triazole

3-bromo-4-(4-chloro-phenyl)-4-oxo-butyric acid ethyl ester

ethyl 4-(4-chlorophenyl)-4-oxobutanoate

Downstream raw materials:

[6-(4-Chloro-phenyl)-3-methyl-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazin-7-yl]-acetic acid

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