7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione

Base Information

Chemical Name:7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione
CAS No.:1365544-69-9
Molecular Formula:C₂₄H₂₄N₂O₇S₂
Molecular Weight:516.596
Hs Code.:

Synonyms:7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione

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Chemical Property of 7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione

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Technology Process of 7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione

There total 6 articles about 7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 39082-53-6
1,1-bis(phenylsulfonyl)ethylene

: 1365544-30-4
5,7-dimethyl-1-vinyl-5,7-diazaspiro[2.5]octane-4,6,8-trione

: 1365544-69-9
7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione

Guidance literature:: With Bu₄N[Fe(CO)3(NO)]; C₂₁H₂₆N₂⁽¹⁺⁾*F₆P^(1-); potassium 2-methylbutan-2-olate; In tetrahydrofuran; toluene; at 80 ℃; for 16h;
DOI:10.1021/ja300294a

Reference yield:

: 3561-67-9
bis(phenylthio)methane

: 1365544-69-9
7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione

Guidance literature:: Multi-step reaction with 4 steps

1: dihydrogen peroxide / acetic anhydride; acetic acid

2: 1,4-dioxane; methanol

3: hydrogenchloride / toluene

4: Bu₄N[Fe(CO)3(NO)]; C₂₁H₂₆N₂⁽¹⁺⁾*F₆P^(1-); potassium 2-methylbutan-2-olate / tetrahydrofuran; toluene / 16 h / 80 °C

With hydrogenchloride; Bu₄N[Fe(CO)3(NO)]; C₂₁H₂₆N₂⁽¹⁺⁾*F₆P^(1-); dihydrogen peroxide; potassium 2-methylbutan-2-olate; In tetrahydrofuran; 1,4-dioxane; methanol; acetic anhydride; acetic acid; toluene;
DOI:10.1021/ja300294a

Reference yield:

: 39837-35-9
1-(2,2-bis(phenylsulfonyl)ethyl)piperidine

: 1365544-69-9
7,9-dimethyl-2,2-bis(phenylsulfonyl)-3-vinyl-7,9-diazaspiro-[4.5]decane-6,8,10-trione

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / toluene

2: Bu₄N[Fe(CO)3(NO)]; C₂₁H₂₆N₂⁽¹⁺⁾*F₆P^(1-); potassium 2-methylbutan-2-olate / tetrahydrofuran; toluene / 16 h / 80 °C

With hydrogenchloride; Bu₄N[Fe(CO)3(NO)]; C₂₁H₂₆N₂⁽¹⁺⁾*F₆P^(1-); potassium 2-methylbutan-2-olate; In tetrahydrofuran; toluene;
DOI:10.1021/ja300294a