N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester
CAS No.:865263-56-5
Molecular Formula:C₃₃H₃₃NO₆
Molecular Weight:539.628
Hs Code.:

Synonyms:N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester

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Chemical Property of N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester

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Technology Process of N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester

There total 3 articles about N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 3,4-dibenzyloxybenzyl iodide

: 54755-77-0
N-benzyloxycarbonyl-3-aminopropionic acid methyl ester

: 865263-56-5
N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester

Guidance literature:: N-benzyloxycarbonyl-3-aminopropionic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

3,4-dibenzyloxybenzyl iodide; In tetrahydrofuran; hexane; at -78 ℃; for 5h;
DOI:10.1016/j.tet.2005.06.094

Reference yield:

: 2304-94-1
3-(benzyloxycarbonylamino)propanoic acid

: 865263-56-5
N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 22.7 g / hydrochloric acid / 0.33 h / Heating

2.1: lithium diisopropylamide / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 53 percent / tetrahydrofuran; hexane / 5 h / -78 °C

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1016/j.tet.2005.06.094

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 865263-56-5
N-benzyloxycarbonyl-2-(3,4-dibenzyloxybenzyl)-3-aminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / 0 - 20 °C

2.1: 22.7 g / hydrochloric acid / 0.33 h / Heating

3.1: lithium diisopropylamide / tetrahydrofuran; hexane / 1 h / -78 °C

3.2: 53 percent / tetrahydrofuran; hexane / 5 h / -78 °C

With hydrogenchloride; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1016/j.tet.2005.06.094