(2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane

Base Information

• Chemical Name: (2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane
• CAS No.: 191481-72-8
• Molecular Formula: C₃₈H₄₂N₂O₅
• Molecular Weight: 606.762

Synonyms:(2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane

Chemical Property of (2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane

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Technology Process of (2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane

There total 2 articles about (2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(Fluoren-9-ylmethoxy-carbonyloxy)-succinimide + (2S,3S,5S)-2-amino-3-hydroxy-5-tert-butoxycarbonylamino-1,6-diphenylhexane succinate (256328-84-4,183388-64-9) → (2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane (191481-72-8)

Guidance literature:

With sodium hydrogencarbonate; In 1,4-dioxane; water; at 25 ℃; for 16h;

Reference yield:

9-fluorenylmethyl-N-succinimidyl carbonate + (2S,3S,5S)-2-amino-3-hydroxy-5-(t-butyloxycarbonylamino)-1,6-diphenylhexane (144163-85-9) → (2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane (191481-72-8) + (2S,3S,5S)-5-[N-[N-((2-pyridinylmethoxy)carbonyl)anthranilyl]amino]2-?N-((3-S-(tetra[hydrofuranyl)oxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane

Guidance literature:

In dichloromethane;

Reference yield:

(2S,3S,5S)-5-[N-(tert-butyloxycarbonyl)amino]-2-[N-((9-fluorenylmethoxy)carbonyl)amino]-1,6-diphenyl-3-hydroxy hexane (191481-72-8) → 9H-fluoren-9-ylmethyl (1S,2S,4S)-4-amino-1-benzyl-2-hydroxy-5-phenylpentylcarbamate hydrochloride (854754-06-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 0 - 25 ℃; for 1h;

upstream raw materials:

(2S,3S,5S)-2-amino-3-hydroxy-5-(t-butyloxycarbonylamino)-1,6-diphenylhexane

(2S,3S,5S)-2-amino-3-hydroxy-5-tert-butoxycarbonylamino-1,6-diphenylhexane succinate

Downstream raw materials:

9H-fluoren-9-ylmethyl (1S,2S,4S)-4-amino-1-benzyl-2-hydroxy-5-phenylpentylcarbamate hydrochloride

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