N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide

Base Information

Chemical Name:N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide
CAS No.:867297-08-3
Molecular Formula:C₂₆H₃₃NO₃S
Molecular Weight:439.619
Hs Code.:

Synonyms:N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide

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Chemical Property of N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide

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Technology Process of N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide

There total 2 articles about N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90841-43-3,16034-99-4
(E)-4-methoxycinnamyl bromide

: 220765-22-0
(4S)-5-methyl-4-[N-(2,4,6-trimethylbenzenesulfonyl)amino]-1,2-hexadiene

: 867297-08-3
N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.1021/jo0700528

Reference yield:

: 53484-50-7
(E)-p-methoxy-cinnamyl alcohol

: 867297-08-3
N-[(1S)-1-isopropylbuta-2,3-dienyl]-N-[(E)-3-(4-methoxyphenyl)prop-2-enyl]-2,4,6-trimethylphenylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / CH₂Cl₂ / 0.5 h / 0 °C

2: 200 mg / NaH / dimethylformamide / 1 h / 0 °C

With phosphorus tribromide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0700528