chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I)

Base Information

• Chemical Name: chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I)
• CAS No.: 1334547-75-9
• Molecular Formula: C₃₅H₅₃AuClO₂P
• Molecular Weight: 769.198

Synonyms:chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I)

Chemical Property of chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I)

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I)

There total 1 articles about chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

chloro(dimethylsulfide) gold(I) (29892-37-3) + dicyclohexyl[3,6-dimethoxy-2′,4′,6′-tris(1-methylethyl)[1,1′-biphenyl]-2-yl]phosphine (1070663-78-3) → chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I) (1334547-75-9)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/acs.orglett.8b03502

Reference yield: 100.0%

chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I) (1334547-75-9) + silver(I) triflimide (189114-61-2) → [BrettPhosAu]NTf2 (1296269-97-0)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/acs.orglett.8b03502

Reference yield: 100.0%

silver hexafluoroantimonate (26042-64-8) + chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl]gold (I) (1334547-75-9) + acetonitrile (75-05-8,26809-02-9) → [BrettPhosAu*MeCN]SbF6

Guidance literature:

In dichloromethane; at 25 ℃; for 8h; Darkness;

DOI:10.1002/chem.201405903

upstream raw materials:

chloro(dimethylsulfide) gold(I)

dicyclohexyl[3,6-dimethoxy-2′,4′,6′-tris(1-methylethyl)[1,1′-biphenyl]-2-yl]phosphine

Downstream raw materials:

{dicyclohexyl[3,6-dimethoxy-2',4',6'-tri(propan-2-yl)biphenyl-2-yl]phosphane-κP}(prop-1-yn-1-yl)gold

[BrettPhosAu]NTf₂

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