2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al

Base Information

• Chemical Name: 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al
• CAS No.: 79936-96-2
• Molecular Formula: C₁₄H₂₂O
• Molecular Weight: 209.304

Synonyms:2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al

Chemical Property of 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al

Chemical Property:

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Technology Process of 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al

There total 2 articles about 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H25(2)H3O2 (79936-76-8) → 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al (79936-96-2)

Guidance literature:

Multi-step reaction with 3 steps

1: conc. HCl / 1.17 h / Heating

2: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

With hydrogenchloride; potassium permanganate; magnesium sulfate; In acetone;

DOI:10.1002/hlca.19810640504

Reference yield:

2-<(1'S,2'S,6'R)-2',6'-dimethyl-2'-(2''-hydroxy-4''-isopropyl)phenyl-6'-triduteriomethyl-cyclohexyl>-essigsauremethylester (79936-77-9) → 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al (79936-96-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

With potassium permanganate; magnesium sulfate; In acetone;

DOI:10.1002/hlca.19810640504

Reference yield: 97.0%

orthoformic acid triethyl ester (122-51-0) + 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al (79936-96-2) → 2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al-diethylacetat (79936-98-4)

Guidance literature:

With toluene-4-sulfonic acid; In ethanol; for 96h;

DOI:10.1002/hlca.19810640504

upstream raw materials:

C₂₀H₂₅⁽²⁾H₃O₂

2-<(1'S,2'S,6'R)-2',6'-dimethyl-2'-(2''-hydroxy-4''-isopropyl)phenyl-6'-triduteriomethyl-cyclohexyl>-essigsauremethylester

Downstream raw materials:

2-methyl-4<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-2'-cyclohexyl>-(E)-2-buten-1-al-diethylacetat

(1R,1'R,6S,6'S)-<16,16,16,16,',16',16'-²H6>-γ,γ-carotin

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