molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′)

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Chemical Name:molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′)
CAS No.:1443767-93-8
Molecular Formula:C₃₀H₂₁MoNO₄P₂
Molecular Weight:617.389
Hs Code.:

Synonyms:molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′)

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Chemical Property of molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′)

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Technology Process of molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′)

There total 2 articles about molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50777-76-9
(2-formylphenyl)(diphenyl)phosphine

: 1443767-93-8
molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′)

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 24 h / Inert atmosphere; Reflux

2: tetrahydrofuran / 24 h / 20 - 40 °C / Inert atmosphere

With toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1039/c3dt50981h

Reference yield:

: 152435-11-5
4-methyl-2-phosphanylaniline

: 1443767-93-8
molybdenum(0)(tetracarbonyl)(2-(2-diphenylphosphanyl)phenyl-5-methyl-1,3-benzazaphosphole-P,P′)

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 24 h / Inert atmosphere; Reflux

2: tetrahydrofuran / 24 h / 20 - 40 °C / Inert atmosphere

With toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1039/c3dt50981h