3-[(3-Furyl)carbonyl]-1-(1-hydroxy-1-methylethyl)-5-methyl-1-cyclohexene

Base Information

Chemical Name:3-[(3-Furyl)carbonyl]-1-(1-hydroxy-1-methylethyl)-5-methyl-1-cyclohexene
CAS No.:68776-18-1
Molecular Formula:C₁₅H₂₀O₃
Molecular Weight:248.322
Hs Code.:
Mol file:68776-18-1.mol

Synonyms:Methanone,3-furanyl[2-(2-hydroxy-2-methylpropylidene)-4-methylcyclopentyl]-, [1S-(1a,2E,4a)]-; Eumorphistonol

Suppliers and Price of 3-[(3-Furyl)carbonyl]-1-(1-hydroxy-1-methylethyl)-5-methyl-1-cyclohexene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3-[(3-Furyl)carbonyl]-1-(1-hydroxy-1-methylethyl)-5-methyl-1-cyclohexene

Chemical Property:

PSA：50.44000
LogP:3.20570

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-[(3-Furyl)carbonyl]-1-(1-hydroxy-1-methylethyl)-5-methyl-1-cyclohexene

There total 5 articles about 3-[(3-Furyl)carbonyl]-1-(1-hydroxy-1-methylethyl)-5-methyl-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 116512-35-7
(1R,4R)-2-(Furan-3-yl-hydroxy-methyl)-4-methyl-1-(2-methyl-propenyl)-cyclopentanol

: 68776-18-1
Furan-3-yl-{(1S,4R)-2-[2-hydroxy-2-methyl-prop-(E)-ylidene]-4-methyl-cyclopentyl}-methanone

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; at -20 ℃;
DOI:10.1016/S0040-4039(00)96802-3

Reference yield:

: 498-60-2
furan-3-carboxaldehyde

: 68776-18-1
Furan-3-yl-{(1S,4R)-2-[2-hydroxy-2-methyl-prop-(E)-ylidene]-4-methyl-cyclopentyl}-methanone

Guidance literature:: Multi-step reaction with 5 steps

2: imidazole

3: H₂ / PtO₂

4: 1.) Me₃CLi, 2.) Bu₄N⁽¹⁺⁾*F^(1-)

5: 15 percent / PDC / dimethylformamide / -20 °C

With 1H-imidazole; dipyridinium dichromate; tetrabutyl ammonium fluoride; hydrogen; tert.-butyl lithium; platinum(IV) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)96802-3

Reference yield:

: 116512-33-5
5-(Furan-3-yl-hydroxy-methyl)-3-methyl-cyclopent-2-enone

: 68776-18-1
Furan-3-yl-{(1S,4R)-2-[2-hydroxy-2-methyl-prop-(E)-ylidene]-4-methyl-cyclopentyl}-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole

2: H₂ / PtO₂

3: 1.) Me₃CLi, 2.) Bu₄N⁽¹⁺⁾*F^(1-)

4: 15 percent / PDC / dimethylformamide / -20 °C

With 1H-imidazole; dipyridinium dichromate; tetrabutyl ammonium fluoride; hydrogen; tert.-butyl lithium; platinum(IV) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)96802-3