(2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid

Base Information

Chemical Name:(2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid
CAS No.:1009036-40-1
Molecular Formula:C₂₄H₄₂O₅Si
Molecular Weight:438.68
Hs Code.:

Synonyms:(2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid

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Chemical Property of (2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid

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Technology Process of (2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid

There total 1 articles about (2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1009036-52-5
C₃₄H₅₁NO₆Si

: 1009036-40-1
(2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid

Guidance literature:: With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 0 - 20 ℃; for 5h;
DOI:10.1021/jo702384d

Reference yield: 79.0%

: 1009036-40-1
(2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid

: 95273-29-3
<3R,4R>-4-methyl-5-hexen-3-ol

: 1009036-41-2
(1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoate

Guidance literature:: (2R,3S,4S,6R)-3-(tert-butyldimethylsilanyloxy)-7-(4-methoxybenzyloxy)-2,4,6-trimethylheptanoic acid; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 3h;

<3R,4R>-4-methyl-5-hexen-3-ol; With dmap; In benzene; at 20 ℃; for 13h; Further stages.;
DOI:10.1021/jo702384d