C₃₇H₄₈O₅Si

Base Information

• Chemical Name: C₃₇H₄₈O₅Si
• CAS No.: 1323858-64-5
• Molecular Formula: C₃₇H₄₈O₅Si
• Molecular Weight: 600.871
• Mol file: 1323858-64-5.mol

Synonyms:C₃₇H₄₈O₅Si

Chemical Property of C₃₇H₄₈O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₄₈O₅Si

There total 11 articles about C₃₇H₄₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C37H46O5Si (1323858-20-3) → C37H48O5Si (1323858-64-5)

Guidance literature:

With sodium tetrahydroborate; nickel(II) chloride heptahydrate; In tetrahydrofuran; methanol; at 0 - 20 ℃;

DOI:10.1002/anie.201101893

Reference yield:

C37H48O5Si (1323858-54-3) → C37H48O5Si (1323858-64-5)

Guidance literature:

Multi-step reaction with 7 steps

1.1: pyridinium p-toluenesulfonate / 20 - 130 °C

2.1: methanol; triethylamine / 14 h / 50 °C

3.1: triethylamine / dichloromethane / 3 h / 0 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

5.1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 0.5 h / 0 °C / Irradiation

6.1: ferrous(II) sulfate heptahydrate; iodine / methanol / 1 h / 20 °C / Inert atmosphere

6.2: 2 h / 80 °C

7.1: sodium tetrahydroborate; nickel(II) chloride heptahydrate / tetrahydrofuran; methanol / 0 - 20 °C

With methanol; ferrous(II) sulfate heptahydrate; sodium tetrahydroborate; lithium aluminium tetrahydride; nickel(II) chloride heptahydrate; iodine; oxygen; pyridinium p-toluenesulfonate; 5,15,10,20-tetraphenylporphyrin; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 5.1: Schenck ene reaction;

DOI:10.1002/anie.201101893

Reference yield:

C39H50O6Si (1323858-56-5) → C37H48O5Si (1323858-64-5)

Guidance literature:

Multi-step reaction with 6 steps

1.1: methanol; triethylamine / 14 h / 50 °C

2.1: triethylamine / dichloromethane / 3 h / 0 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

4.1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 0.5 h / 0 °C / Irradiation

5.1: ferrous(II) sulfate heptahydrate; iodine / methanol / 1 h / 20 °C / Inert atmosphere

5.2: 2 h / 80 °C

6.1: sodium tetrahydroborate; nickel(II) chloride heptahydrate / tetrahydrofuran; methanol / 0 - 20 °C

With methanol; ferrous(II) sulfate heptahydrate; sodium tetrahydroborate; lithium aluminium tetrahydride; nickel(II) chloride heptahydrate; iodine; oxygen; 5,15,10,20-tetraphenylporphyrin; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 4.1: Schenck ene reaction;

DOI:10.1002/anie.201101893

upstream raw materials:

C₃₇H₄₈O₅Si

C₃₉H₅₀O₆Si

C₃₇H₄₈O₄Si

C₃₇H₄₈O₆Si

Downstream raw materials:

C₃₇H₅₂O₅Si