2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride

Base Information

Chemical Name:2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride
CAS No.:1225025-56-8
Molecular Formula:C₂₅H₃₁O₅PSi*ClH
Molecular Weight:507.038
Hs Code.:

Synonyms:2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride

Chemical Property:

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Technology Process of 2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride

There total 8 articles about 2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₅O₇PSi

: 1225025-56-8
2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃; for 1.5h;

Reference yield:

: 2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenyl methoxymethyl ether

: 1225025-56-8
2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃; for 1.5h; Further stages;

Reference yield:

: 151-10-0
1,3-Dimethoxybenzene

: 1225025-56-8
2-bis(2,6-dimethoxyphenyl)phosphano-6-(trimethylsilyl)phenol hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium; iodine / hexane; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: isopropylmagnesium chloride / tetrahydrofuran / 1 h / -50 - 20 °C

3: phosphorus trichloride / tetrahydrofuran / -78 - 20 °C

4: n-butyllithium / hexane; tetrahydrofuran / 2 h / 0 - 20 °C

5: hydrogenchloride / ethyl acetate / 1.5 h / 0 - 20 °C

With hydrogenchloride; n-butyllithium; iodine; isopropylmagnesium chloride; phosphorus trichloride; In tetrahydrofuran; hexane; ethyl acetate;