trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester
CAS No.:861930-69-0
Molecular Formula:C₃₂H₃₀F₃NO₆S
Molecular Weight:613.655
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

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Chemical Property of trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

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Technology Process of trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

There total 1 articles about trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 861930-70-3
trifluoro-methanesulfonic acid 6-hydroxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

: 100-51-6,185532-71-2
benzyl alcohol

: 861930-69-0
trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

Guidance literature:: With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield: 60.0%

: 861930-69-0
trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

: 1993-03-9
o-fluorophenylboronic acid

: [6-benzyloxy-2-(2-fluoro-phenyl)-naphthalen-1-yl]-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone

Guidance literature:: trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester; o-fluorophenylboronic acid; bis-triphenylphosphine-palladium(II) chloride; In acetonitrile;

With cesium fluoride; at 75 ℃; for 1h;

Reference yield: 36.0%

: 861930-69-0
trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

: 861931-76-2
(2-{6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl}-5-fluoro-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: tert-butyl N-(2-bromo-5-fluorophenyl)carbamate; With bis(pinacol)diborane; tricyclohexylphosphine; palladium diacetate; In acetonitrile; at 20 ℃; for 0.0833333h;

With cesium fluoride; at 20 - 90 ℃; for 0.5 - 0.75h;

trifluoromethanesulfonic acid 6-benzyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester; at 90 ℃; for 4h;