2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine

Base Information

Chemical Name:2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine
CAS No.:1292287-57-0
Molecular Formula:C₁₉H₁₂ClFN₄O₃
Molecular Weight:398.781
Hs Code.:

Synonyms:2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine

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Chemical Property of 2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine

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Technology Process of 2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine

There total 2 articles about 2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1292287-58-1
4-(2-amino-phenylamino)-5-chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-pyrimidine

: 1292287-57-0
2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine

: 1292287-56-9
2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-5,10-dihydro-benzo[g]pteridine

Guidance literature:: With water; sodium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,2-dimethoxyethane; at 150 ℃; for 1h; Microwave irradiation;

Reference yield:

: 1165931-74-7
2-(4-chloro-2-fluoro-3-methoxyphenyl)-4,5-dichloro-6-methoxycarbonyl-pyrimidine

: 95-54-5
1,2-diamino-benzene

: 1292287-57-0
2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-benzo[g]pteridine

: 1292287-56-9
2-(4-chloro-2-fluoro-3-methoxyphenyl)-4-methoxycarbonyl-5,10-dihydro-benzo[g]pteridine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dimethyl sulfoxide / 3 h / 90 °C

2: water; sodium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,2-dimethoxyethane / 1 h / 150 °C / Microwave irradiation

With water; sodium carbonate; triethylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,2-dimethoxyethane; dimethyl sulfoxide;