2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside

Base Information

• Chemical Name: 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside
• CAS No.: 117252-78-5
• Molecular Formula: C₆₈H₇₄O₂₆Si
• Molecular Weight: 1335.41

Synonyms:2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside

Chemical Property of 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside

There total 1 articles about 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

acetic anhydride (108-24-7) + 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-<2,3-di-O-benzoyl-4-O-α-D-galactopyranosyl-β-D-galactopyranosyl>-β-D-glucopyranoside (117253-36-8) → 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside (117252-78-5)

Guidance literature:

With pyridine;

DOI:10.1021/jo00259a006

Reference yield: 96.0%

2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside (117252-78-5) → 2,3,6-tri-O-benzoyl-4-O-<6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-α-D-glucopyranosyl chloride (126257-37-2)

Guidance literature:

With Dichloromethyl methyl ether; zinc(II) chloride; In chloroform; for 19h;

DOI:10.1021/jo00297a038

Reference yield:

2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside (117252-78-5) + acetic anhydride (108-24-7) → 1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-<6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β/α-D-glucopyranose (117252-87-6,117253-45-9)

Guidance literature:

With boron trifluoride diethyl etherate; In toluene; at 22 ℃; for 15h; Yield given;

DOI:10.1021/jo00259a006

upstream raw materials:

acetic anhydride

2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-<2,3-di-O-benzoyl-4-O-α-D-galactopyranosyl-β-D-galactopyranosyl>-β-D-glucopyranoside

Downstream raw materials:

2,3,6-tri-O-benzoyl-4-O-<6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-α-D-glucopyranosyl chloride

1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-<6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β/α-D-glucopyranose

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 117252-78-5 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzoyl-4-O-[6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl]-β-D-glucopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send