C₃₀H₂₈N₂O₆

Base Information

Chemical Name:C₃₀H₂₈N₂O₆
CAS No.:1402730-61-3
Molecular Formula:C₃₀H₂₈N₂O₆
Molecular Weight:512.562
Hs Code.:

C<sub>30</sub>H<sub>28</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₀H₂₈N₂O₆

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Chemical Property of C₃₀H₂₈N₂O₆

Chemical Property:

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Technology Process of C₃₀H₂₈N₂O₆

There total 10 articles about C₃₀H₂₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 120-72-9
indole

: 1402730-60-2
2-[5-(benzyloxymethyl)-3-hydroxy-3-(methoxycarbonyl)tetrahydrofuran-2-yl]-3-oxo-3H-indole 1-oxide

: 1402730-61-3
C₃₀H₂₈N₂O₆

Guidance literature:: With indium(III) chloride; In acetonitrile; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201103604

Reference yield:

: 1402730-54-4
8-(benzyloxymethyl)-6-ethynyl-2,2-dimethyl-1,3,7-trioxaspiro[4.4]nonane

: 1402730-61-3
C₃₀H₂₈N₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / 8 h / 0 - 20 °C

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 6 h / Reflux

4: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 10 h / 20 °C

5: methanol; hexane; toluene / 0.33 h / 0 °C

6: dichloro bis(acetonitrile) palladium(II) / acetonitrile / 8 h / 20 °C / Inert atmosphere

7: indium(III) chloride / acetonitrile / 5 h / 20 °C / Inert atmosphere

With indium(III) chloride; bis-triphenylphosphine-palladium(II) chloride; dichloro bis(acetonitrile) palladium(II); sodium chlorite; copper(l) iodide; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; hexane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 1: Sonogashira coupling;
DOI:10.1002/chem.201103604

Reference yield:

: 78687-63-5
2,6-O-isopropylidene-α-D-glucoisosaccharino-1,4-lactone

: 1402730-61-3
C₃₀H₂₈N₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1H-imidazole / dichloromethane / 4 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 1 h / -78 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 °C

4.2: 3 h / 0 °C

5.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / methanol / 8 h / 0 - 20 °C

7.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 6 h / Reflux

8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 10 h / 20 °C

9.1: methanol; hexane; toluene / 0.33 h / 0 °C

10.1: dichloro bis(acetonitrile) palladium(II) / acetonitrile / 8 h / 20 °C / Inert atmosphere

11.1: indium(III) chloride / acetonitrile / 5 h / 20 °C / Inert atmosphere

With 1H-imidazole; triethylsilane; indium(III) chloride; bis-triphenylphosphine-palladium(II) chloride; dichloro bis(acetonitrile) palladium(II); sodium chlorite; copper(l) iodide; n-butyllithium; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; boron trifluoride diethyl etherate; sodium hydride; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 5.1: Sonogashira coupling;
DOI:10.1002/chem.201103604