C₂₂H₁₉N₇O₅S

Base Information

Chemical Name:C₂₂H₁₉N₇O₅S
CAS No.:1429313-66-5
Molecular Formula:C₂₂H₁₉N₇O₅S
Molecular Weight:493.503
Hs Code.:

C<sub>22</sub>H<sub>19</sub>N<sub>7</sub>O<sub>5</sub>S

Synonyms:C₂₂H₁₉N₇O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₉N₇O₅S

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Technology Process of C₂₂H₁₉N₇O₅S

There total 9 articles about C₂₂H₁₉N₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 1429313-65-4
C₂₂H₂₁N₇O₆S

: 1429313-66-5
C₂₂H₁₉N₇O₅S

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 1429313-60-9
C₁₉H₂₁BrN₆O₆S

: 1429313-66-5
C₂₂H₁₉N₇O₅S

Guidance literature:: Multi-step reaction with 6 steps

1: dmap / tetrahydrofuran / 5 h / 55 °C

2: XPhos; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere

3: hydrogenchloride / methanol / 2 h / 20 °C

4: caesium carbonate / 50 °C

5: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 2 h / 20 °C

6: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogenchloride; dmap; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium hydroxide monohydrate; water; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1429313-62-1
C₃₅H₄₃N₇O₁₀S

: 1429313-66-5
C₂₂H₁₉N₇O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / methanol / 2 h / 20 °C

2: caesium carbonate / 50 °C

3: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 2 h / 20 °C

4: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogenchloride; lithium hydroxide monohydrate; water; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;