diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate

Base Information

Chemical Name:diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate
CAS No.:1438387-42-8
Molecular Formula:C₂₂H₃₁NO₄P₂
Molecular Weight:435.44
Hs Code.:

Synonyms:diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate

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Chemical Property of diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate

Chemical Property:

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Technology Process of diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate

There total 8 articles about diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₁NO₃P₂

: 1438387-42-8
diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate

Guidance literature:: With dihydrogen peroxide; In water; acetone; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2013.04.005

Reference yield:

: 38318-52-4
α-bromovinylphosphonic acid diethyl ester

: 1438387-42-8
diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: Inert atmosphere

2: triethylamine / dichloromethane / 20 °C

3: tetrahydrofuran / 4.75 h / -78 °C

4: dihydrogen peroxide / acetone; water / 1 h / 20 °C

With dihydrogen peroxide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1016/j.tetasy.2013.04.005

Reference yield:

: 682-30-4
Diethyl vinylphosphonate

: 1438387-42-8
diethyl ((R)-1-((R)-1-(diphenylphosphoryl)butan-2-yl)aziridin-2-yl)phosphonate

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / 0 °C

2: triethylamine

3: Inert atmosphere

4: triethylamine / dichloromethane / 20 °C

5: tetrahydrofuran / 4.75 h / -78 °C

6: dihydrogen peroxide / acetone; water / 1 h / 20 °C

With dihydrogen peroxide; bromine; triethylamine; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1016/j.tetasy.2013.04.005