N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin

Base Information

Chemical Name:N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin
CAS No.:105404-87-3
Molecular Formula:C₃₁H₃₁ClN₂
Molecular Weight:467.054
Hs Code.:

Synonyms:N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin

Chemical Property:

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Technology Process of N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin

There total 4 articles about N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 105378-77-6
1-<2-(4-Chlorphenylethyl)>-4-phenylpiperidin-4-yl-methanamin

: 66-99-9
β-naphthaldehyde

: 105404-87-3
N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 3h; Heating;
DOI:10.1002/ardp.19863190606

Reference yield:

: 40481-13-8
4-phenyl-4-cyanopiperidine

: 105404-87-3
N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent

2: 75 percent / LiAlH₄ / tetrahydrofuran

3: 75 percent / p-toluenesulfonic acid / toluene / 3 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1002/ardp.19863190606

Reference yield:

: 105378-94-7
1-(4-Cyano-4-phenylpiperidin-1-yl)-2-(4-chlorphenyl)-1-ethanon

: 105404-87-3
N-<1-<2-(4-Chlorphenyl)-ethyl>-4-phenylpiperidin-4-yl>-2-naphthylmethanimin

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / LiAlH₄ / tetrahydrofuran

2: 75 percent / p-toluenesulfonic acid / toluene / 3 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1002/ardp.19863190606