1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin

Base Information

• Chemical Name: 1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin
• CAS No.: 1254120-91-6
• Molecular Formula: C₄₄H₄₀O₇
• Molecular Weight: 680.797
• Mol file: 1254120-91-6.mol

Synonyms:1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin

Chemical Property of 1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin

Chemical Property:

Purity/Quality:

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Technology Process of 1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin

There total 1 articles about 1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

bis(p-methoxyphenyl)methanone (90-96-0) + (RS)-1,11-dibromo-5,7-dihydrodibenzoxepin (121772-87-0) → 1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin (1254120-91-6)

Guidance literature:

(RS)-1,11-dibromo-5,7-dihydrodibenzoxepin; With tert.-butyl lithium;

bis(p-methoxyphenyl)methanone;

DOI:10.1039/c0cc00026d

Reference yield: 97.0%

1,11-bis[bis(4-methoxyphenyl)hydroxymethyl]-5,7-dihydrodibenz[c,e]oxepin (1254120-91-6) → 5,7-dihydrodibenz[c,e]oxepin-1,11-diylbis[bis(4-methoxyphenyl)methylium] ditetrafluoroborate

Guidance literature:

With tetrafluoroboric acid; trifluoroacetic anhydride;

DOI:10.1039/c0cc00026d

upstream raw materials:

bis(p-methoxyphenyl)methanone

(RS)-1,11-dibromo-5,7-dihydrodibenzoxepin