Technology Process of 3-benzyloxy-4-methoxy-2-(3-methylbut-2-enyl)benzaldehyde
There total 4 articles about 3-benzyloxy-4-methoxy-2-(3-methylbut-2-enyl)benzaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 23 percent / potassium carbonate, potassium iodide / acetone / 65 h / Heating
2: 91 percent / H2 / Lindlar catalyst / ethyl acetate / 20 °C
3: 86 percent / 0.1 h / 135 °C
4: 83 percent / potassium carbonate, potassium iodide / acetone / 16 h / Heating
With
hydrogen; potassium carbonate; potassium iodide;
Lindlar's catalyst;
In
ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / H2 / Lindlar catalyst / ethyl acetate / 20 °C
2: 86 percent / 0.1 h / 135 °C
3: 83 percent / potassium carbonate, potassium iodide / acetone / 16 h / Heating
With
hydrogen; potassium carbonate; potassium iodide;
Lindlar's catalyst;
In
ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: zinc bromide / CH2Cl2 / 20 °C
2: 23 percent / potassium carbonate, potassium iodide / acetone / 65 h / Heating
3: 91 percent / H2 / Lindlar catalyst / ethyl acetate / 20 °C
4: 86 percent / 0.1 h / 135 °C
5: 83 percent / potassium carbonate, potassium iodide / acetone / 16 h / Heating
With
hydrogen; potassium carbonate; potassium iodide; zinc dibromide;
Lindlar's catalyst;
In
dichloromethane; ethyl acetate; acetone;
