Technology Process of C22H28O4
There total 8 articles about C22H28O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
at -40 - 20 ℃;
for 1.83333h;
regioselective reaction;
Inert atmosphere;
DOI:10.1021/ol102390t
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / -10 - 20 °C / Inert atmosphere
2: titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N-Diisopropyltryptamine / decane; dichloromethane / -30 - -25 °C / Molecular sieve; Inert atmosphere
3: tetrahydrofuran / 1.83 h / -40 - 20 °C / Inert atmosphere
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium aluminium tetrahydride; N,N-Diisopropyltryptamine;
In
tetrahydrofuran; decane; dichloromethane;
2: Sharpless epoxidation;
DOI:10.1021/ol102390t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N-Diisopropyltryptamine / decane; dichloromethane / -30 - -25 °C / Molecular sieve; Inert atmosphere
2: tetrahydrofuran / 1.83 h / -40 - 20 °C / Inert atmosphere
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N-Diisopropyltryptamine;
In
tetrahydrofuran; decane; dichloromethane;
1: Sharpless epoxidation;
DOI:10.1021/ol102390t
