C₁₃H₁₄O₂

Base Information

Chemical Name:C₁₃H₁₄O₂
CAS No.:908592-00-7
Molecular Formula:C₁₃H₁₄O₂
Molecular Weight:202.253
Hs Code.:

C<sub>13</sub>H<sub>14</sub>O<sub>2</sub>

Synonyms:C₁₃H₁₄O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₄O₂

Chemical Property:

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Technology Process of C₁₃H₁₄O₂

There total 3 articles about C₁₃H₁₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₄O₂

: 908592-01-8
C₁₃H₁₄O₂

: 908592-00-7
C₁₃H₁₄O₂

Guidance literature:: With trimethylphosphane; In tert-butyl alcohol; at 20 ℃; for 18h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.061

Reference yield:

: 908591-99-1
C₁₃H₁₄O₂

: 908592-01-8
C₁₃H₁₄O₂

: 908592-00-7
C₁₃H₁₄O₂

Guidance literature:: With trimethylphosphane; In tert-butyl alcohol; at 20 ℃; for 18h; Title compound not separated from byproducts.;
DOI:10.1039/b603510h

Reference yield:

: 495-41-0
1-phenylbut-2-en-1-one

: 908592-01-8
C₁₃H₁₄O₂

: 908592-00-7
C₁₃H₁₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 18 h / Inert atmosphere; Reflux

2: trimethylphosphane / tert-butyl alcohol / 18 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; trimethylphosphane; In dichloromethane; tert-butyl alcohol; 2: Morita-Baylis-Hillman type reaction;
DOI:10.1016/j.tet.2011.09.061