1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane

Base Information

Chemical Name:1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane
CAS No.:1240790-19-5
Molecular Formula:C₂₄H₃₃BO₃
Molecular Weight:380.335
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane

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Chemical Property of 1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane

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Technology Process of 1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane

There total 10 articles about 1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: {1,3-bis[2,6-bis(propan-2-yl)phenyl]-2,3-dihydro-1H-imidazol-2-yl}[5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentyl]copper

: 1240790-19-5
1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In toluene; at 45 ℃; for 6h; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.9b02372

Reference yield: 85.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1823-14-9
5-phenyl-1-pentyne

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1240790-19-5
1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane

Guidance literature:: 5-phenyl-1-pentyne; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With [1,3-bis(2,6-di-iso-propylphenyl)imidazol-2-ylidene]copper(I) tert-butoxide; potassium tert-butylate; In toluene; at 45 ℃; Inert atmosphere; Glovebox;

1-bromo-4-methoxy-benzene; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In toluene; at 45 ℃; for 6h; Reagent/catalyst; Solvent; regioselective reaction; Catalytic behavior; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.9b02372

Reference yield: 75.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1172611-54-9
2,2'-(4-phenylpentane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 1240790-19-5
1-(4-methoxyphenyl)-5-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentane

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium hydroxide; In 1,4-dioxane; water; at 25 ℃; for 6h; chemoselective reaction;
DOI:10.1021/ja105176v