C₃₇H₄₉NO₂SSn

Base Information

Chemical Name:C₃₇H₄₉NO₂SSn
CAS No.:1421265-52-2
Molecular Formula:C₃₇H₄₉NO₂SSn
Molecular Weight:690.578
Hs Code.:

C<sub>37</sub>H<sub>49</sub>NO<sub>2</sub>SSn

Synonyms:C₃₇H₄₉NO₂SSn

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Chemical Property of C₃₇H₄₉NO₂SSn

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Technology Process of C₃₇H₄₉NO₂SSn

There total 1 articles about C₃₇H₄₉NO₂SSn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1092363-75-1
N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

: 1421265-52-2
C₃₇H₄₉NO₂SSn

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / Reflux; Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 - -50 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; In tetrahydrofuran; hexane; toluene; 1.1: |Stille Cross Coupling;
DOI:10.1016/j.tet.2012.12.071

Reference yield: 64.0%

: 1071224-34-4
7-bromobenzo[c][1,2,5]thiadiazole-4-carboxaldehyde

: 1421265-52-2
C₃₇H₄₉NO₂SSn

: 1421265-55-5
7-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)benzo[c][1,2,5]thiadiazole-4-carbaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2012.12.071

Reference yield:

: 1421265-52-2
C₃₇H₄₉NO₂SSn

: 1421265-60-2
C₄₄H₄₄N₄O₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 110 °C / Inert atmosphere

2: piperidine / chloroform / 12 h / Reflux; Inert atmosphere

With piperidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In chloroform; toluene; 1: |Stille Cross Coupling / 2: |Knoevenagel Condensation;
DOI:10.1016/j.tet.2012.12.071