Technology Process of C16H20I2O
There total 3 articles about C16H20I2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,3-di(but-3-ynyl)-2-methoxy-5-methylbenzene;
With
Schwartz's reagent;
In
dichloromethane;
at 20 ℃;
for 0.25h;
Inert atmosphere;
Darkness;
With
iodine;
In
dichloromethane;
for 0.5h;
Inert atmosphere;
Darkness;
DOI:10.1002/anie.201206785
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / methanol / 5 h / 20 °C / Inert atmosphere
2.1: Schwartz's reagent / dichloromethane / 0.25 h / 20 °C / Inert atmosphere; Darkness
2.2: 0.5 h / Inert atmosphere; Darkness
With
Schwartz's reagent; potassium carbonate;
In
methanol; dichloromethane;
DOI:10.1002/anie.201206785
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium diacetate; tetrabutyl-ammonium chloride; lithium acetate / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere; Schlenk technique
2.1: potassium carbonate / methanol / 5 h / 20 °C / Inert atmosphere
3.1: Schwartz's reagent / dichloromethane / 0.25 h / 20 °C / Inert atmosphere; Darkness
3.2: 0.5 h / Inert atmosphere; Darkness
With
Schwartz's reagent; lithium acetate; tetrabutyl-ammonium chloride; palladium diacetate; potassium carbonate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
1.1: |Heck Reaction;
DOI:10.1002/anie.201206785
