5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione

Base Information

Chemical Name:5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione
CAS No.:24192-67-4
Molecular Formula:C₁₉H₁₈N₂O₂
Molecular Weight:306.364
Hs Code.:

Synonyms:5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione

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Chemical Property of 5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione

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Technology Process of 5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione

There total 4 articles about 5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 24192-67-4
5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione

Guidance literature:: With tert.-butylhydroperoxide; tris(1,10-phenanthroline)iron(III) tris(hexafluorophosphate); In acetonitrile; at 20 ℃; for 12h; Inert atmosphere; Sealed tube;

Reference yield: 81.0%

: 941-69-5
N-phenyl-maleimide

: 613-97-8
N-methyl-N-ethylaniline

: 24192-67-4
5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione

Guidance literature:: With eosin Y disodium salt; In 1,4-dioxane; at 20 ℃; for 24h; regioselective reaction; Irradiation;
DOI:10.1016/j.tet.2020.131891

Reference yield:

: 100-61-8
N-methylaniline

: 24192-67-4
5-ethyl-2-phenyl-3a,4,5,9b-tetrahydro-1H-pyrrolo[3,4-c]quinoline-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

2: eosin Y disodium salt / 1,4-dioxane / 24 h / 20 °C / Irradiation

With potassium carbonate; eosin Y disodium salt; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2020.131891