(1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine

Base Information

Chemical Name:(1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine
CAS No.:84995-12-0
Molecular Formula:C₄₄H₅₆N₂O₂
Molecular Weight:644.941
Hs Code.:

Synonyms:(1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine

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Technology Process of (1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine

There total 5 articles about (1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 35132-20-8
(R,R)-1,2-diphenylethylenediamine

: 84995-12-0
(1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine

Guidance literature:: In ethanol; for 18h; Reflux;
DOI:10.1055/s-2008-1077900

Reference yield:

: 1073145-36-4
C₁₄H₁₆N₂*C₄H₆O₆

: 84995-12-0
(1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water / 20 °C

2: ethanol / 2.5 h / 20 °C / Reflux

With potassium carbonate; In ethanol; water;
DOI:10.1021/ma301696d

Reference yield:

: 5700-60-7
1,2-Diphenylethylenediamine

: 84995-12-0
(1R,2R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-diphenylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: L-Tartaric acid

1.2: 20 °C

2.1: ethanol / 2.5 h / 20 °C / Reflux

With L-Tartaric acid; In ethanol;
DOI:10.1021/ma301696d