benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate

Base Information

Chemical Name:benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate
CAS No.:634614-27-0
Molecular Formula:C₁₉H₂₅N₃O₄
Molecular Weight:359.425
Hs Code.:

Synonyms:benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate

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Chemical Property of benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate

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Technology Process of benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate

There total 1 articles about benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 634614-26-9
1-benzyl-4-methyl-(4R)-3-(6-cyanohexyl)-2-oxoimidazolidine-1,4-dicarboxylate

: 634614-27-0
benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate

Guidance literature:: 1-benzyl-4-methyl-(4R)-3-(6-cyanohexyl)-2-oxoimidazolidine-1,4-dicarboxylate; With sodium tetrahydroborate; In methanol; at -20 - 20 ℃; for 2h;

With hydrogenchloride; water;

Reference yield:

: 634614-27-0
benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate

: 634614-28-1
benzyl (4R)-3-(6-cyanohexyl)-4-formyl-2-oxoimidazolidine-1-carboxylate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 634614-27-0
benzyl(4R)-3-(6-cyanohexyl)-4-(hydroxymethyl)-2-oxoimidazolidine-1-carboxylate

: 634614-31-6
(5S)-5-[(1E)-3-hydroxy-4-phenylbut-1-enyl]-1-[6-(1H-tetraazol-5-yl)hexyl]imidazolidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2.2: 3 h / 0 - 20 °C

3.1: sodium tetrahydroborate / 1 h / -20 - 20 °C

4.1: azido tributyltin (IV) / 3 h / 100 °C

4.2: 24 h / 25 °C

With sodium tetrahydroborate; sodium hydride; Dess-Martin periodane; azido tributyltin (IV); In tetrahydrofuran; dichloromethane;