(3-(2,2-Diethoxyethoxy)phenyl)boronic acid

Base Information

Chemical Name:(3-(2,2-Diethoxyethoxy)phenyl)boronic acid
CAS No.:312931-07-0
Molecular Formula:C₁₂H₁₉BO₅
Molecular Weight:254.091
Hs Code.:
DSSTox Substance ID:DTXSID601257428

Synonyms:312931-07-0;(3-(2,2-Diethoxyethoxy)phenyl)boronic acid;SCHEMBL1785537;DTXSID601257428;B-[3-(2,2-Diethoxyethoxy)phenyl]boronic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-(2,2-Diethoxyethoxy)phenyl)boronic acid

Chemical Property:

Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:254.1325539
Heavy Atom Count:18
Complexity:209

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B(C1=CC(=CC=C1)OCC(OCC)OCC)(O)O

Technology Process of (3-(2,2-Diethoxyethoxy)phenyl)boronic acid

There total 1 articles about (3-(2,2-Diethoxyethoxy)phenyl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 312931-07-0
(3-{[2,2-Bis(ethyloxy)ethyl]oxy}phenyl)boronic acid

Guidance literature:

Reference yield:

: 5751-82-6
ethyl 5‐chlorothiophene‐2‐carboxylate

: 312931-07-0
(3-{[2,2-Bis(ethyloxy)ethyl]oxy}phenyl)boronic acid

: 1007578-47-3
ethyl 5-(3-{[2,2-bis(ethyloxy)ethyl]oxy}phenyl)-2-thiophene carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In acetonitrile; at 90 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: 312931-07-0
(3-{[2,2-Bis(ethyloxy)ethyl]oxy}phenyl)boronic acid

: 1007578-71-3
ethyl 5-{3-[(2-oxoethyl)oxy]phenyl}-2-thiophenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / acetonitrile / 2.5 h / 90 °C / Inert atmosphere

2: trifluoroacetic acid / water; chloroform / 21 h / 0 - 65 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trifluoroacetic acid; In chloroform; water; acetonitrile;