(2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane

Base Information

Chemical Name:(2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane
CAS No.:1005001-53-5
Molecular Formula:C₁₇H₁₉N₃O₃
Molecular Weight:313.356
Hs Code.:

Synonyms:(2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane

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Technology Process of (2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane

There total 3 articles about (2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 115584-73-1
p-phenylazobenzoic acid N-hydroxysuccinimidyl ester

: 44520-55-0
D-threoninol

: 1005001-53-5
(2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane

Guidance literature:: With dmap; In ethyl acetate; for 0.166667h; chemoselective reaction; Vibration ball-milling;
DOI:10.1039/c1gc15131b

Reference yield:

: 98-95-3,26969-40-4
nitrobenzene

: 1005001-53-5
(2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 24 h / 20 °C

2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 °C

With benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1039/c7cc04599a

Reference yield:

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1005001-53-5
(2S,3S)-(2-N-(p-phenylazo)benzamido)-1,3-dihydroxybutane

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 24 h / 20 °C

2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 °C

With benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1039/c7cc04599a