9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one

Base Information

Chemical Name:9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one
CAS No.:951923-60-7
Molecular Formula:C₁₆H₁₆N₆O₃
Molecular Weight:340.341
Hs Code.:

Synonyms:9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one

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Technology Process of 9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one

There total 2 articles about 9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 4418-61-5
5-aminotetrazole

: 555-16-8
4-nitrobenzaldehdye

: 126-81-8
dimedone

: 951923-60-7
9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one

Guidance literature:: With polyethylene glycol (PEG)-400; at 110 ℃; for 0.5h; Microwave irradiation; Green chemistry;
DOI:10.1080/00397911.2019.1659973

Reference yield: 67.0%

: 7,7-dimethyl-4-(4-nitrophenyl)-2-thioxo-2,3,4,6,7,8-hexahydro-1H-quinazolin-5-one

: 951923-60-7
9-(4-nitrophenyl)-6,6-dimethyl-5,6,7,9-tetrahydrotetrazolo[5,1-b]quinazolin-8(4H)-one

Guidance literature:: With sodium azide; mercury(II) diacetate; In acetic acid; at 100 ℃; for 6h; regioselective reaction;
DOI:10.3987/COM-11-12351