(Z)-9-Anthracenecarbaldehyde oxime

Base Information

• Chemical Name: (Z)-9-Anthracenecarbaldehyde oxime
• CAS No.: 2497-53-2
• Molecular Formula: C₁₅H₁₁NO
• Molecular Weight: 221.258
• Mol file: 2497-53-2.mol

Synonyms:(Z)-anthracene-9-carbaldehyde oxime

Chemical Property of (Z)-9-Anthracenecarbaldehyde oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (Z)-9-Anthracenecarbaldehyde oxime

There total 4 articles about (Z)-9-Anthracenecarbaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

9-anthracene aldehyde (642-31-9) → (Z)-anthracene-9-carbaldehyde oxime (2497-53-2)

Guidance literature:

With hydroxylamine hydrochloride; sodium carbonate; In ethanol; for 0.25h; Heating;

DOI:10.1135/cccc20020665

Reference yield:

9-anthracene aldehyde (642-31-9) → (Z)-anthracene-9-carbaldehyde oxime (2497-53-2)

Guidance literature:

With ethanol; sodium carbonate;

DOI:10.1021/ja01277a079

Reference yield:

9-(1-hydroxyethyl)anthracene (74928-67-9,94942-50-4,114128-93-7,7512-20-1) → (Z)-anthracene-9-carbaldehyde oxime (2497-53-2)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium; carbon disulfide; methyl iodide / weiteres Reagens: Xylol; weitere Angaben: Destillation des Reaktionsprodukts unter vermindertem Druck

2: POCl₃; 1.2-dichloro-benzene / 90 - 95 °C

3: ethanol; Na₂CO₃

With carbon disulfide; ethanol; sodium; sodium carbonate; 1,2-dichloro-benzene; trichlorophosphate; methyl iodide;

DOI:10.1021/ja01277a079

upstream raw materials:

9-anthracene aldehyde

9-(1-hydroxyethyl)anthracene

anthracene

Downstream raw materials:

anthracene-9-carbaldehyde-((E)-O-acetyl oxime )

(E)‐anthracene‐9‐carbaldehyde oxime

9-cyanoanthracene

Refernces