((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine

Base Information

Chemical Name:((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine
CAS No.:1312540-17-2
Molecular Formula:C₃₃H₃₇O₂PS
Molecular Weight:528.695
Hs Code.:

Synonyms:((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine

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Technology Process of ((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine

There total 3 articles about ((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1312540-18-3
(1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-ol

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1312540-17-2
((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine

Guidance literature:: With dmap; triethylamine; In toluene; at 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.050

Reference yield:

: 287929-74-2
(2S,3S)-(+)-(2,4,6-timethylphenyl)oxirane-2-methanol

: 1312540-17-2
((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / -20 °C / Inert atmosphere

1.2: 5 h / -20 - 20 °C / Inert atmosphere

2.1: sodium hydroxide / 1,4-dioxane; water / 2 h / 80 °C

3.1: dmap; triethylamine / toluene / 0.33 h / 20 °C / Inert atmosphere

With dmap; sodium hydride; triethylamine; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2011.04.050

Reference yield:

: 1221576-36-8
(2S,3S)-2-mesityl-3-(methoxymethyl)oxirane

: 1312540-17-2
((1R,2S)-1-(3,5-dimethylphenylthio)-1-mesityl-3-methoxypropan-2-yloxy)diphenylphosphine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / 1,4-dioxane; water / 2 h / 80 °C

2: dmap; triethylamine / toluene / 0.33 h / 20 °C / Inert atmosphere

With dmap; triethylamine; sodium hydroxide; In 1,4-dioxane; water; toluene;
DOI:10.1016/j.tet.2011.04.050