2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine

Base Information

Chemical Name:2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine
CAS No.:72874-59-0
Molecular Formula:C₁₈H₁₆BrN₅
Molecular Weight:382.263
Hs Code.:

Synonyms:2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine

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Chemical Property of 2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine

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Technology Process of 2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine

There total 4 articles about 2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.7%

: 60640-15-5
8-bromo-1-(2-phthalimidoethyl)-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine

: 72874-59-0
2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine

Guidance literature:: With methylamine; In ethanol; dichloromethane; at 0 - 20 ℃; for 25h;
DOI:10.1021/jm00178a009

Reference yield:

: 72874-57-8
7-bromo-2-hydrazino-5-phenyl-3H-[1,4]benzodiazepine

: 72874-59-0
2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) carbonyldiimidazole / 1.) THF, RT, 72 min, 2.) THF, RT, 18 h

2: acetic acid / 0.7 h / 117 °C

3: 80.7 percent / 40percent aq. MeNH₂ / ethanol; CH₂Cl₂ / 25 h / 0 - 20 °C

With 1,1'-carbonyldiimidazole; methylamine; In ethanol; dichloromethane; acetic acid;
DOI:10.1021/jm00178a009

Reference yield:

: 3-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propionic acid N'-(7-bromo-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl)-hydrazide

: 72874-59-0
2-(8-Bromo-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 0.7 h / 117 °C

2: 80.7 percent / 40percent aq. MeNH₂ / ethanol; CH₂Cl₂ / 25 h / 0 - 20 °C

With methylamine; In ethanol; dichloromethane; acetic acid;
DOI:10.1021/jm00178a009