C₁₅H₁₅NO₂

Base Information

• Chemical Name: C₁₅H₁₅NO₂
• CAS No.: 1428865-36-4
• Molecular Formula: C₁₅H₁₅NO₂
• Molecular Weight: 241.29
• Mol file: 1428865-36-4.mol

Synonyms:C₁₅H₁₅NO₂

Chemical Property of C₁₅H₁₅NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₅NO₂

There total 5 articles about C₁₅H₁₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H17NO2 (1428865-24-0) → C15H15NO2 (1428865-36-4)

Guidance literature:

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethyl acetate; at 100 ℃; for 3h;

DOI:10.1021/ol400371h

Reference yield:

aniline (62-53-3) → C15H15NO2 (1428865-36-4)

Guidance literature:

Multi-step reaction with 4 steps

1.1: copper diacetate; sodium acetate / water / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / Cooling with ice

2.2: 2 h / 80 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 100 °C

With lithium aluminium tetrahydride; copper diacetate; sodium acetate; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1021/ol400371h

Reference yield:

C16H17NO3 (1428865-11-5) → C15H15NO2 (1428865-36-4)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 100 °C

With lithium aluminium tetrahydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethyl acetate;

DOI:10.1021/ol400371h

upstream raw materials:

aniline

C₁₅H₁₇NO₂

C₁₆H₁₇NO₃

2-anilino-3-methoxy-benzoic acid

Refernces