1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole

Base Information

Chemical Name:1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole
CAS No.:324519-47-3
Molecular Formula:C₂₀H₂₁N₃O₆
Molecular Weight:399.403
Hs Code.:

Synonyms:1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole

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Chemical Property of 1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole

Chemical Property:

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Technology Process of 1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole

There total 4 articles about 1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 324519-47-3
1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / 10-camphorsulfonic acid / 16 h / 65 °C

2: 69 percent / POCl₃; Et₃N / 1,2-dimethoxy-ethane / 3 h / -5 °C

3: K₂CO₃ / ethanol; methanol; 1,2-dimethoxy-ethane / 6 h / Heating

With (1S)-10-camphorsulfonic acid; potassium carbonate; triethylamine; trichlorophosphate; In methanol; 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jm010523x

Reference yield:

: 31680-08-7
4-methoxy-3-nitrobenzaldehyde

: 324519-47-3
1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / ethanol; methanol / 2 h / Heating

2: K₂CO₃ / ethanol; methanol; 1,2-dimethoxy-ethane / 6 h / Heating

With potassium carbonate; acetic acid; In methanol; 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jm010523x

Reference yield:

: 324519-53-1
N-{[(4-methylphenyl)sulfonyl](3,4,5-trimethoxyphenyl)methyl}formamide

: 324519-47-3
1-methyl-4-(3,4,5-trimethoxyphenyl)-5-(3-nitro-4-methoxyphenyl)imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / POCl₃; Et₃N / 1,2-dimethoxy-ethane / 3 h / -5 °C

2: K₂CO₃ / ethanol; methanol; 1,2-dimethoxy-ethane / 6 h / Heating

With potassium carbonate; triethylamine; trichlorophosphate; In methanol; 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jm010523x