N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide

Base Information

• Chemical Name: N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide
• CAS No.: 115961-17-6
• Molecular Formula: C₂₂H₂₅NO₅S₂
• Molecular Weight: 447.576

Synonyms:N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide

Chemical Property of N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide

There total 6 articles about N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

4,N-Dimethyl-N-[2-(6-oxo-2-phenylsulfanyl-cyclohex-1-enyl)-ethyl]-benzenesulfonamide → N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide (115961-17-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 25 ℃; for 16h;

DOI:10.1021/jo00255a008

Reference yield: 82.0%

sodium benzenesulfonate (873-55-2) + Methanesulfonic acid 2-{2-[methyl-(toluene-4-sulfonyl)-amino]-ethyl}-3-oxo-cyclohex-1-enyl ester (115960-86-6) → N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide (115961-17-6)

Guidance literature:

With 1-methyl-pyrrolidin-2-one; at 25 ℃; for 192h;

DOI:10.1021/jo00255a008

Reference yield:

N-(p-toluenesulfonyl)aziridine (3634-89-7) → N-[2-(2-Benzenesulfonyl-6-oxo-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide (115961-17-6)

Guidance literature:

Multi-step reaction with 5 steps

3: aq.HCl

With hydrogenchloride;

DOI:10.1021/jo00194a051

upstream raw materials:

sodium benzenesulfonate

Methanesulfonic acid 2-{2-[methyl-(toluene-4-sulfonyl)-amino]-ethyl}-3-oxo-cyclohex-1-enyl ester

N-(p-toluenesulfonyl)aziridine

Downstream raw materials:

N-[2-(2-Benzenesulfonyl-6-hydroxy-cyclohex-1-enyl)-ethyl]-4,N-dimethyl-benzenesulfonamide

N-{2-[2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-cyclohexa-1,5-dienyl]-ethyl}-4,N-dimethyl-benzenesulfonamide

Methanesulfonic acid 3-benzenesulfonyl-2-{2-[methyl-(toluene-4-sulfonyl)-amino]-ethyl}-cyclohex-2-enyl ester

N-{2-[6-Benzenesulfonyl-2-(2-methoxy-5-vinyl-phenoxy)-cyclohex-1-enyl]-ethyl}-4,N-dimethyl-benzenesulfonamide

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