C₂₉H₃₈N₂O₅

Base Information

Chemical Name:C₂₉H₃₈N₂O₅
CAS No.:1343505-47-4
Molecular Formula:C₂₉H₃₈N₂O₅
Molecular Weight:494.631
Hs Code.:

C<sub>29</sub>H<sub>38</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₉H₃₈N₂O₅

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Chemical Property of C₂₉H₃₈N₂O₅

Chemical Property:

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Technology Process of C₂₉H₃₈N₂O₅

There total 15 articles about C₂₉H₃₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₄₀N₂O₆

: 1343505-47-4
C₂₉H₃₈N₂O₅

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 72h;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-16-7
C₁₈H₂₈O₄

: 1343505-47-4
C₂₉H₃₈N₂O₅

Guidance literature:: Multi-step reaction with 12 steps

1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

3: triethylamine / dichloromethane / 0 - 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

5: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / dichloromethane / 7 h / 0 - 20 °C

6: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

7: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

8: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

9: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

10: water; lithium hydroxide / tert-butyl alcohol

11: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

12: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; N,N-dimethyl-formamide / 72 h / 0 - 20 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; dmap; sodium chlorite; 1-hydroxy-7-aza-benzotriazole; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; tetrabutyl ammonium fluoride; water; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-03-2
C₂₄H₄₄O₄Si

: 1343505-47-4
C₂₉H₃₈N₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

3: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / dichloromethane / 7 h / 0 - 20 °C

4: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

5: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

6: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

7: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

8: water; lithium hydroxide / tert-butyl alcohol

9: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

10: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; N,N-dimethyl-formamide / 72 h / 0 - 20 °C

With 1-ethyl-piperidine; dmap; sodium chlorite; 1-hydroxy-7-aza-benzotriazole; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; tetrabutyl ammonium fluoride; water; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158