cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

Base Information

Chemical Name:cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester
CAS No.:242483-27-8
Molecular Formula:C₂₃H₂₈OS₃
Molecular Weight:416.673
Hs Code.:

cyclohexanecarbothioic acid <i>S</i>-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

Synonyms:cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

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Chemical Property of cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

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Technology Process of cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

There total 4 articles about cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2719-27-9
cyclohexanylcarbonyl chloride

: 242483-19-8
4,4-Bis(phenylthio)-2-butanethiol

: 242483-27-8
cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1055/s-1999-2777

Reference yield:

: 3561-67-9
bis(phenylthio)methane

: 242483-27-8
cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / BuLi / tetrahydrofuran / 0.25 h / 0 °C

2: pyridine / 0 - 20 °C

3: 1.) K⁽¹⁺⁾*t-BuOCHS₂^(1-) / 2.) 70-80 deg C

4: 78 percent / Et₃N / tetrahydrofuran / 0 - 20 °C

With pyridine; n-butyllithium; K⁽¹⁺⁾*t-BuOCHS₂^(1-); triethylamine; In tetrahydrofuran;
DOI:10.1055/s-1999-2777

Reference yield:

: 185559-30-2
4,4-Bis-phenylsulfanyl-butan-2-ol

: 242483-27-8
cyclohexanecarbothioic acid S-(1-methyl-3,3-bis-phenylsulfanyl-propyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C

2: 1.) K⁽¹⁺⁾*t-BuOCHS₂^(1-) / 2.) 70-80 deg C

3: 78 percent / Et₃N / tetrahydrofuran / 0 - 20 °C

With pyridine; K⁽¹⁺⁾*t-BuOCHS₂^(1-); triethylamine; In tetrahydrofuran;
DOI:10.1055/s-1999-2777