Technology Process of C27H27N3O3
There total 7 articles about C27H27N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
water; N,N-dimethyl-formamide;
at 100 ℃;
for 6h;
Inert atmosphere;
DOI:10.1016/j.bmc.2012.09.048
- Guidance literature:
-
Multi-step reaction with 5 steps
1: manganese(IV) oxide / acetone / 20 °C / Inert atmosphere
2: dmap / tetrahydrofuran; hexane / 1 h / 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
4: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere
5: sodium iodide / N,N-dimethyl-formamide; water / 6 h / 100 °C / Inert atmosphere
With
dmap; manganese(IV) oxide; tetrabutyl ammonium fluoride; potassium carbonate; sodium iodide;
In
tetrahydrofuran; hexane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2012.09.048
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere
3: sodium iodide / N,N-dimethyl-formamide; water / 6 h / 100 °C / Inert atmosphere
With
tetrabutyl ammonium fluoride; potassium carbonate; sodium iodide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.09.048
