(S)-5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-1H-imidazo<4.5-c>pyridine-6-carboxylic acid

Base Information

Chemical Name:(S)-5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-1H-imidazo<4.5-c>pyridine-6-carboxylic acid
CAS No.:114786-33-3
Molecular Formula:C₃₄H₂₉N₃O₃
Molecular Weight:527.623
Hs Code.:

Synonyms:(S)-5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-1H-imidazo<4.5-c>pyridine-6-carboxylic acid

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Chemical Property of (S)-5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-1H-imidazo<4.5-c>pyridine-6-carboxylic acid

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Technology Process of (S)-5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-1H-imidazo<4.5-c>pyridine-6-carboxylic acid

There total 11 articles about (S)-5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-1H-imidazo<4.5-c>pyridine-6-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 133808-03-4
(S)-1-Benzhydryl-5-diphenylacetyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridine-6-carboxylic acid methyl ester

: 114786-33-3
(S)-5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-1H-imidazo<4.5-c>pyridine-6-carboxylic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; for 2h; Ambient temperature;
DOI:10.1002/jhet.5570280118

Reference yield:

: 133808-03-4
1-Benzhydryl-5-diphenylacetyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridine-6-carboxylic acid methyl ester

: 114786-33-3
1H-Imidazo[4,5-c]pyridine-6-carboxylic acid, 5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; Ambient temperature;
DOI:10.1021/jm00115a014

Reference yield:

: (S)-3-(2-Oxo-2-phenyl-ethyl)-4,5,6,7-tetrahydro-3H-imidazo[4,5-c]pyridine-6-carboxylic acid methyl ester

: 114786-33-3
1H-Imidazo[4,5-c]pyridine-6-carboxylic acid, 5-(diphenylacetyl)-1-(diphenylmethyl)-4,5,6,7-tetrahydro-

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide (DCC), hydroxybenztriazole (HOBT*H₂O) / dimethylformamide

2: 2.) glacial AcOH, Zn / 1.) CH₃CN, reflux, 2.) MeOH, sonication, 2 h

3: 1 N NaOH / tetrahydrofuran; methanol / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; zinc; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00115a014