Cyclopropanecarboxylic acid, 1-[(ethoxycarbonyl)amino]-2-fluoro-, methyl ester (9CI)

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 1-[(ethoxycarbonyl)amino]-2-fluoro-, methyl ester (9CI)
CAS No.:188897-48-5
Molecular Formula:C₈H₁₂FNO₄
Molecular Weight:205.186
Hs Code.:
Mol file:188897-48-5.mol

Synonyms:Cyclopropanecarboxylic acid, 1-[(ethoxycarbonyl)amino]-2-fluoro-, methyl ester (9CI)

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Chemical Property of Cyclopropanecarboxylic acid, 1-[(ethoxycarbonyl)amino]-2-fluoro-, methyl ester (9CI)

Chemical Property:

PSA：64.63000
LogP:0.77700

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarboxylic acid, 1-[(ethoxycarbonyl)amino]-2-fluoro-, methyl ester (9CI)

There total 2 articles about Cyclopropanecarboxylic acid, 1-[(ethoxycarbonyl)amino]-2-fluoro-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 188897-46-3
1-Ethoxycarbonylamino-2-fluoro-cyclopropanecarboxylic acid

: 188897-48-5
1-Ethoxycarbonylamino-2-fluoro-cyclopropanecarboxylic acid methyl ester

Guidance literature:: In diethyl ether; at 0 ℃; for 1h;
DOI:10.1016/S0040-4039(97)00199-8

Reference yield:

: 188897-44-1
[1-(3,4-Dimethoxy-phenyl)-2-fluoro-cyclopropyl]-carbamic acid ethyl ester

: 188897-48-5
1-Ethoxycarbonylamino-2-fluoro-cyclopropanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: O₃ / CH₂Cl₂ / 0.25 h

2: H₂O₂ / 1 h / Heating

3: 96 percent / diethyl ether / 1 h / 0 °C

With dihydrogen peroxide; ozone; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(97)00199-8