1-methyl-N-(4-methyl cyclohexylidene)-ethylamine

Base Information

• Chemical Name: 1-methyl-N-(4-methyl cyclohexylidene)-ethylamine
• CAS No.: 53451-22-2
• Molecular Formula: C₁₀H₁₉N
• Molecular Weight: 153.268

Synonyms:1-methyl-N-(4-methyl cyclohexylidene)-ethylamine

Chemical Property of 1-methyl-N-(4-methyl cyclohexylidene)-ethylamine

Chemical Property:

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Technology Process of 1-methyl-N-(4-methyl cyclohexylidene)-ethylamine

There total 1 articles about 1-methyl-N-(4-methyl cyclohexylidene)-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-methylcyclohexan-4-one (589-92-4) + isopropylamine (75-31-0) → 1-methyl-N-(4-methyl cyclohexylidene)-ethylamine (53451-22-2)

Guidance literature:

With titanium tetrachloride; In diethyl ether; for 5h; Heating;

DOI:10.1016/0040-4020(96)00046-4

Reference yield:

1-methyl-N-(4-methyl cyclohexylidene)-ethylamine (53451-22-2) → 5-methyl-1H-indole (614-96-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) LDA, 3.) K₂CO₃, 4.) (COOH)2*2H₂O, NaOH

2: 10percent Pd/C / o-xylene / 48 h / Heating

With sodium hydroxide; palladium on activated charcoal; oxalic acid; potassium carbonate; lithium diisopropyl amide; In o-xylene;

DOI:10.1016/0040-4020(96)00046-4

Reference yield:

1-methyl-N-(4-methyl cyclohexylidene)-ethylamine (53451-22-2) → C10H21N (1260245-97-3) + C10H21N (1260245-93-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 26 ℃; for 96h;

DOI:10.1002/mrc.2693

upstream raw materials:

1-methylcyclohexan-4-one

isopropylamine

Downstream raw materials:

5-methyl-1H-indole

C₁₀H₂₁N

C₁₀H₂₁N

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