2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline

Base Information

• Chemical Name: 2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline
• CAS No.: 78179-08-5
• Molecular Formula: C₁₉H₂₀N₂O₅
• Molecular Weight: 356.378

Synonyms:2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline

Chemical Property of 2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of 2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline

There total 1 articles about 2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-methoxy-2-nitrotoluene (4837-88-1) + 6-methyl-7,8-dihydro-[1,3]dioxolo[4,5-g]isoquinolin-6-ium iodide (35287-11-7) → 2,2'-dimethyl-3,3'-dimethoxyazoxybenzene (78179-10-9) + 2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline (78179-08-5)

Guidance literature:

With sodium ethanolate; In ethanol; 1) warming, 15 min, 2) overnight;

Reference yield:

2-methyl-1-(2'-nitro-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline (78179-08-5) → 2-methyl-1-(2'-amino-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline (78179-09-6)

Guidance literature:

With hydrogen; platinum(IV) oxide; In methanol; for 6h; under 2068.6 Torr;

upstream raw materials:

6-methoxy-2-nitrotoluene

6-methyl-7,8-dihydro-[1,3]dioxolo[4,5-g]isoquinolin-6-ium iodide

Downstream raw materials:

2-methyl-1-(2'-amino-6'-methoxybenzyl)-6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline

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