3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid]

Base Information

Chemical Name:3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid]
CAS No.:1206717-17-0
Molecular Formula:C₄₄H₅₂N₄O₁₂
Molecular Weight:828.916
Hs Code.:

Synonyms:3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid]

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Chemical Property of 3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid]

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Technology Process of 3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid]

There total 1 articles about 3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1206717-16-9
tetramethyl 3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoate]

: 1206717-17-0
3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid]

Guidance literature:: With potassium hydroxide; In methanol; water; for 16h;
DOI:10.1002/hlca.200900161

Reference yield: 71.0%

: 1206717-17-0
3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxybenzoic acid]

: 2627-86-3
(S)-1-phenyl-ethylamine

: 3,3',3'',3'''-[1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetrakis(methylene)]tetrakis[2-methoxy-N-[(1R)-1-phenylethyl]carboxamide]

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; for 7h; Inert atmosphere; Cooling with ice;
DOI:10.1002/hlca.200900161