4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline

Base Information

Chemical Name:4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline
CAS No.:60418-42-0
Molecular Formula:C₁₃H₁₆N₆
Molecular Weight:256.31
Hs Code.:

4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-<i>N</i>,<i>N</i>-dimethyl-aniline

Synonyms:4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline

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Chemical Property of 4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline

Chemical Property:

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Technology Process of 4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline

There total 10 articles about 4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-73-3
3-Nitrochlorobenzene

: 60418-42-0
4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / fuming nitric acid, 98percent sulphuric acid / 1 h / 30 °C

2: 76 percent / urea, hydrazine hydrate / ethanol

3: 74 percent / 98percent sulphuric acid / ethanol; acetic acid / 6 h / Heating

4: 96 percent / sodium hydrogencarbonate, pyridine / H₂O / Heating

5: 98 percent / hydrogen / Raney nickel / ethanol

6: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide, sodium acetate / 1.) water, 0 deg C, 2.) 1 h

With pyridine; hydrogenchloride; sodium azide; sulfuric acid; hydrogen; nitric acid; sodium acetate; sodium hydrogencarbonate; hydrazine hydrate; urea; sodium nitrite; nickel; In ethanol; water; acetic acid;
DOI:10.1039/P19800000982

Reference yield:

: 585-79-5
m-nitrobromobenzene

: 60418-42-0
4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / fuming nitric acid, 98percent sulphuric acid / 1 h / 30 °C

2: urea, hydrazine hydrate / ethanol

3: 68 percent / 98percent sulphuric acid / ethanol; acetic acid / 6 h / Heating

4: 96 percent / sodium hydrogencarbonate, pyridine / H₂O / Heating

5: 98 percent / hydrogen / Raney nickel / ethanol

6: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide, sodium acetate / 1.) water, 0 deg C, 2.) 1 h

With pyridine; hydrogenchloride; sodium azide; sulfuric acid; hydrogen; nitric acid; sodium acetate; sodium hydrogencarbonate; hydrazine hydrate; urea; sodium nitrite; nickel; In ethanol; water; acetic acid;
DOI:10.1039/P19800000982

Reference yield:

: 610-38-8
4-bromo-1,2-dinitrobenzene

: 60418-42-0
4-azido-3-(3,5-dimethyl-pyrazol-1-yl)-N,N-dimethyl-aniline

Guidance literature:: Multi-step reaction with 5 steps

1: urea, hydrazine hydrate / ethanol

2: 68 percent / 98percent sulphuric acid / ethanol; acetic acid / 6 h / Heating

3: 96 percent / sodium hydrogencarbonate, pyridine / H₂O / Heating

4: 98 percent / hydrogen / Raney nickel / ethanol

5: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide, sodium acetate / 1.) water, 0 deg C, 2.) 1 h

With pyridine; hydrogenchloride; sodium azide; sulfuric acid; hydrogen; sodium acetate; sodium hydrogencarbonate; hydrazine hydrate; urea; sodium nitrite; nickel; In ethanol; water; acetic acid;
DOI:10.1039/P19800000982