dihydroguaiaretic acid dimethyl ether

Base Information

• Chemical Name: dihydroguaiaretic acid dimethyl ether
• CAS No.: 119182-23-9
• Molecular Formula: C₂₂H₃₀O₄
• Molecular Weight: 358.478

Synonyms:dihydroguaiaretic acid dimethyl ether

Chemical Property of dihydroguaiaretic acid dimethyl ether

Chemical Property:

Purity/Quality:

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Technology Process of dihydroguaiaretic acid dimethyl ether

There total 20 articles about dihydroguaiaretic acid dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C22H28O4 (278808-07-4) → 2,3-bis[(3,4-dimethoxyphenyl)methyl]butane (5701-82-6,24150-24-1,68930-18-7,119182-23-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate; for 1h;

DOI:10.1016/S0040-4039(01)01182-0

Reference yield: 100.0%

(8R,8R')-3,4,3',4'-tetramethoxylignan-9,9'-diyl bis(methanesulfonate) (119098-90-7) → dihydroguaiaretic acid dimethyl ether (119182-23-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Heating;

Reference yield: 0.4%

Nordihydroguaiaretic acid (119584-40-6,27686-84-6,741285-10-9) + dimethyl sulfate (77-78-1) → dihydroguaiaretic acid dimethyl ether (119182-23-9)

Guidance literature:

With potassium carbonate; In acetone; for 6h; Heating;

DOI:10.1021/jo00292a010

upstream raw materials:

(8R,8R')-3,4,3',4'-tetramethoxylignan-9,9'-diyl bis(methanesulfonate)

Nordihydroguaiaretic acid

dimethyl sulfate

dimethylmatairesinol

Downstream raw materials:

C₁₈H₂₂O₄

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